Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

Base Information

Chemical Name:Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate
CAS No.:1381785-31-4
Molecular Formula:C₂₃H₁₆F₄N₃O₅S*Na
Molecular Weight:545.447
Hs Code.:

Synonyms:Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

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Chemical Property of Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

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Technology Process of Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

There total 7 articles about Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1381785-29-0
Methyl 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

: 1381785-31-4
Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: With sodium hydroxide; In methanol; for 24h; Reflux;

Reference yield:

: 1381785-47-2
6-Fluoro-3-methylimidazo[1,2-a]pyridine-2-carbohydrazide

: 1381785-31-4
Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / Cooling with ice

2.1: 18 h / Reflux

3.1: sodium hydride / ethyl acetate; N,N-dimethyl-formamide; mineral oil / 20 °C / Cooling with ice

3.2: 18 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

6.1: sodium hydroxide / methanol / 24 h / Reflux

With hydrogenchloride; sodium hydride; potassium carbonate; sodium hydroxide; sodium nitrite; In 1,4-dioxane; methanol; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1381785-46-1
2-Amino-1-(4-ethoxy-3,4-dioxobutan-2-yl)-5-fluoropyridin-1-ium bromide

: 1381785-31-4
Sodium 4-(N-(6-fluoro-3-methylimidazo[1,2-a]pyridin-2-yl)-N-(4-(trifluoromethoxy)benzyl)sulfamoyl)benzoate

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol / 6 h / Reflux

2.1: hydrazine / ethanol / 72 h / Reflux

3.1: hydrogenchloride; sodium nitrite / water / 0.5 h / Cooling with ice

4.1: 18 h / Reflux

5.1: sodium hydride / ethyl acetate; N,N-dimethyl-formamide; mineral oil / 20 °C / Cooling with ice

5.2: 18 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 18 h / 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

8.1: sodium hydroxide / methanol / 24 h / Reflux

With hydrogenchloride; sodium hydride; potassium carbonate; sodium hydroxide; hydrazine; sodium nitrite; In 1,4-dioxane; methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;