(1S,2R)-2-amino-1,2-diphenylethanol hydrochloride

Base Information

Chemical Name:(1S,2R)-2-amino-1,2-diphenylethanol hydrochloride
CAS No.:131298-18-5
Molecular Formula:C₁₄H₁₅NO*ClH
Molecular Weight:249.74
Hs Code.:

Synonyms:(1S,2R)-2-amino-1,2-diphenylethanol hydrochloride

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Chemical Property of (1S,2R)-2-amino-1,2-diphenylethanol hydrochloride

Chemical Property:

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Technology Process of (1S,2R)-2-amino-1,2-diphenylethanol hydrochloride

There total 2 articles about (1S,2R)-2-amino-1,2-diphenylethanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (±)-2-((diphenylmethylene)amino)-1,2-diphenylethan-1-ol

: 5959-42-2,14149-03-2,39664-83-0,88784-88-7,100423-12-9,100423-13-0,131298-18-5
(+/-)-erythro-α'-amino-bibenzyl-α-ol; hydrochloride

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; at 60 ℃; for 0.5h; pH=< 4;
DOI:10.1021/acs.oprd.8b00133

Reference yield:

: 1689-71-0,17619-97-5,25144-18-7,38628-70-5,40102-60-1,1439-07-2
2,3-diphenyloxirane

: 5959-42-2,14149-03-2,39664-83-0,88784-88-7,100423-12-9,100423-13-0,131298-18-5
(+/-)-erythro-α'-amino-bibenzyl-α-ol; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: yttrium(III) trifluoromethanesulfonate / acetonitrile / 20 h / 60 °C / Sealed tube

2: hydrogenchloride / water; ethyl acetate / 0.5 h / 60 °C / pH < 4

With hydrogenchloride; yttrium(III) trifluoromethanesulfonate; In water; ethyl acetate; acetonitrile;
DOI:10.1021/acs.oprd.8b00133

Reference yield:

: 131298-18-5
(1S,2R)-2-amino-1,2-diphenylethanol hydrochloride

: 530-36-9,3764-63-4,13286-63-0,23190-16-1,23190-17-2,23364-44-5,23412-95-5,39664-87-4,88082-66-0
(1R,2R)-2-amino-1,2-diphenylethane-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 150 °C

2: 1) SOCl₂, 2) H⁺ / 2) H₂O

With thionyl chloride; hydrogen cation;