methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

Base Information

• Chemical Name: methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate
• CAS No.: 1012860-69-3
• Molecular Formula: C₃₈H₄₄O₁₂
• Molecular Weight: 692.76

Synonyms:methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

Chemical Property of methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

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Technology Process of methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

There total 2 articles about methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-67-1) → methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-69-3)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 96h;

DOI:10.1016/j.carres.2007.10.030

Reference yield: 44.0%

benzyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-68-2) → methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-69-3) + methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-67-1) + benzyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-70-6)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 77.5h;

DOI:10.1016/j.carres.2007.10.030

Reference yield: 39.0%

methyl (4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-69-3) + methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-2,3-di-O-benzyl-α-D-galactopyranosyluronate trichloroacetimidate (1012860-73-9) → methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosyluronate)-(1->2)-(4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate (1012860-77-3)

Guidance literature:

With silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 17h;

DOI:10.1016/j.carres.2007.10.030

upstream raw materials:

methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

benzyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

Downstream raw materials:

methyl (2-O-acetyl-4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosyluronate)-(1->2)-(4-O-allyl-3-O-benzoyl-α-L-rhamnopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-α-D-galactopyranosid)uronate

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