2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

Base Information

Chemical Name:2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione
CAS No.:1438435-23-4
Molecular Formula:C₂₂H₂₈O₅
Molecular Weight:372.461
Hs Code.:

Synonyms:2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

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Chemical Property of 2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

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Technology Process of 2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

There total 1 articles about 2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 73194-08-8
2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

: 89358-30-5
benzyl (2E)-4-bromobut-2-en-1-yl ether

: 1438435-23-4
2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

Guidance literature:: 2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h; Inert atmosphere;

benzyl (2E)-4-bromobut-2-en-1-yl ether; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201200499

Reference yield:

: 1438435-23-4
2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

: C₁₅H₂₂O₅

Guidance literature:: With hydrogen; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/adsc.201200499

Reference yield:

: 1438435-23-4
2-(4-Benzyloxy-2-butenyl)-2-[2-(ethoxycarbonyl)ethyl]-1,3-cyclohexanedione

: 1438435-24-5
2-[2-(ethoxycarbonyl)ethyl]-2-(4-hydroxybutyl)-1,3-cyclohexanedione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol;
DOI:10.1002/adsc.201200499