N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

Base Information

Chemical Name:N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine
CAS No.:1146622-60-7
Molecular Formula:C₃₁H₃₅N₅O₂
Molecular Weight:509.651
Hs Code.:

N<sub>1</sub>-(tert-butoxycarbonyl)-N<sub>2</sub>-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

Synonyms:N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

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Technology Process of N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

There total 4 articles about N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1146622-74-3
N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

: 1146622-60-7
N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h;
DOI:10.1021/jm9000693

Reference yield:

: 194985-14-3
N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)guanidine

: 152030-49-4
3-(1-trityl-1H-imidazol-4-yl)propan-1-ol

: 1146622-60-7
N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

: 1146622-59-4
N-(tert-butoxycarbonyl)-N-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

Guidance literature:: N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)guanidine; 3-(1-trityl-1H-imidazol-4-yl)propan-1-ol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h;
DOI:10.1021/jm9000693

Reference yield:

: 194985-13-2
BocHNC(SMe)=NCbz

: 1146622-60-7
N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; mercury dichloride / dichloromethane / 48 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; methanol / 20 °C / 6000.6 Torr

With palladium 10% on activated carbon; hydrogen; triethylamine; mercury dichloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm201128q