C₂₂H₂₈N₂O₃S₃

Base Information

Chemical Name:C₂₂H₂₈N₂O₃S₃
CAS No.:142867-82-1
Molecular Formula:C₂₂H₂₈N₂O₃S₃
Molecular Weight:464.674
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>S<sub>3</sub>

Synonyms:C₂₂H₂₈N₂O₃S₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₈N₂O₃S₃

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Technology Process of C₂₂H₂₈N₂O₃S₃

There total 5 articles about C₂₂H₂₈N₂O₃S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 142867-81-0
C₁₅H₂₂N₂O₃S₃

: 142867-82-1
C₂₂H₂₈N₂O₃S₃

Guidance literature:: With trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1021/ja00044a008

Reference yield:

: 142867-79-6
C₁₄H₂₀N₂O₄S₃

: 142867-82-1
C₂₂H₂₈N₂O₃S₃

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 0.5 h / Ambient temperature

2: Pb(OAc)4 / ethyl acetate / 0.17 h / Ambient temperature

3: NaBH₄ / methanol / 0.5 h / 0 °C

4: 63 percent / 4 Angstroem molecular sieves, trifluoromethanesulfonic acid / CH₂Cl₂ / 10 h / Ambient temperature

With lead(IV) acetate; sodium tetrahydroborate; trifluorormethanesulfonic acid; 4 A molecular sieve; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00044a008

Reference yield:

: C₁₅H₂₀N₂O₃S₃

: 142867-82-1
C₂₂H₂₈N₂O₃S₃

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 0.5 h / 0 °C

2: 63 percent / 4 Angstroem molecular sieves, trifluoromethanesulfonic acid / CH₂Cl₂ / 10 h / Ambient temperature

With sodium tetrahydroborate; trifluorormethanesulfonic acid; 4 A molecular sieve; In methanol; dichloromethane;
DOI:10.1021/ja00044a008