(2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

Base Information

Chemical Name:(2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester
CAS No.:1333925-94-2
Molecular Formula:C₁₈H₂₀F₃NO₇
Molecular Weight:419.355
Hs Code.:

Synonyms:(2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

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Chemical Property of (2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

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Technology Process of (2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

There total 2 articles about (2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 136194-92-8
(S)-2-allyloxycarbonylamino-3-hydroxypropionic acid methyl ester

: 1333925-94-2
(2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol202270g

Reference yield:

: 1333925-60-2
(S)-2-allyloxycarbonylamino-3-allyloxycarbonyloxypropionic acid methyl ester

: 1333925-94-2
(2S,2'S)-3,3,3-trifluoro-2-methoxy-2-phenylpropionic acid (2'-allyloxycarbonyl-2'-methoxycarbonylethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: [Bu₄N][Fe(CO)3(NO)]; tris(2,4,6-trimethylphenyl)phosphine / ethanol / 40 °C / Inert atmosphere

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; [Bu₄N][Fe(CO)3(NO)]; tris(2,4,6-trimethylphenyl)phosphine; In ethanol; dichloromethane;
DOI:10.1021/ol202270g