1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

Base Information

Chemical Name:1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl
CAS No.:1446527-26-9
Molecular Formula:C₃₄H₂₉N₄O₅
Molecular Weight:573.628
Hs Code.:

Synonyms:1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

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Chemical Property of 1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

Chemical Property:

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Technology Process of 1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

There total 8 articles about 1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1446527-25-8
1-(4-benzoyloxyphenyl)-5-(4-hydroxyphenyl)-3-phenyl-6-oxoverdazyl

: 2719-27-9
cyclohexanylcarbonyl chloride

: 1446527-26-9
1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1021/jo400843y

Reference yield:

: 4-benzoyloxyphenylhydrazine hydrochloride

: 1446527-26-9
1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

Guidance literature:: Multi-step reaction with 6 steps

1: ethanol / 0 - 20 °C

2: pyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: triethylamine / ethanol / 50 °C

4: CN^(1-)*Fe⁽³⁺⁾*K⁽¹⁺⁾; sodium carbonate; tetrabutylammomium bromide / dichloromethane / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethanol; tetrahydrofuran / 24 h / 2585.81 Torr

6: pyridine / dichloromethane / 0.17 h / 20 °C

With pyridine; CN^(1-)*Fe⁽³⁺⁾*K⁽¹⁺⁾; palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; sodium carbonate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo400843y

Reference yield:

: 1446527-15-6
1-(4-benzoyloxyphenyl)-5-(4-benzyloxyphenyl)-3-phenyl-6-oxoverdazyl

: 1446527-26-9
1-(4-benzoyloxyphenyl)-5-(4-(cyclohexylcarbonyloxy)phenyl)-3-phenyl-6-oxoverdazyl

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol; tetrahydrofuran / 24 h / 2585.81 Torr

2: pyridine / dichloromethane / 0.17 h / 20 °C

With pyridine; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo400843y