B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

Base Information

Chemical Name:B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃
CAS No.:1227007-93-3
Molecular Formula:C₁₈H₃₄B₁₀O
Molecular Weight:374.577
Hs Code.:

B<sub>10</sub>H<sub>10</sub>CC<sub>7</sub>H<sub>15</sub>CCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>COCH<sub>3</sub>

Synonyms:B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

Suppliers and Price of B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

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Technology Process of B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

There total 1 articles about B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1227007-92-2
B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

: 108-24-7
acetic anhydride

: 1227007-93-3
B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

Guidance literature:: With ethyl(diisopropyl)amine; LiCl; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In dimethylformamide; (Ar) acetic anhydride, Pd-complex, amine-compound and LiCl were added toa soln. of carborane-compound in DME, the mixt. was stirred at 100.degr ee.C for 20 h, cooled to room temp.; filtered thorugh a silica gel pad, quenched with water, extd. with diethyl ether, the organic layer was dried over MgSO4, evapd., silica gel chromy. with 30% ethyl acetate in hexane as eluent; as oil: elem. anal.;
DOI:10.1021/ja101845m