2,3,3,3-Tetrafluoro-1-phenylpropan-1-one

Base Information

• Chemical Name: 2,3,3,3-Tetrafluoro-1-phenylpropan-1-one
• CAS No.: 2267-65-4
• Molecular Formula: C₉H₆F₄O
• Molecular Weight: 206.14
• Hs Code.: 2914700090
• DSSTox Substance ID: DTXSID70505552
• Mol file: 2267-65-4.mol

Synonyms:2267-65-4;2,3,3,3-Tetrafluoro-1-phenylpropan-1-one;DTXSID70505552;MGVPMFSYZYUVSV-UHFFFAOYSA-N;2,3,3,3-tetrafluoropropiophenone;1-Propanone, 2,3,3,3-tetrafluoro-1-phenyl-?;1-Propanone,2,3,3,3-tetrafluoro-1-phenyl-(9ci)

Chemical Property of 2,3,3,3-Tetrafluoro-1-phenylpropan-1-one

Chemical Property:

• PSA: 17.07000
• LogP: 2.76970
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 206.03547746
• Heavy Atom Count: 14
• Complexity: 205

Purity/Quality:

99% ^*data from raw suppliers

1-PROPANONE, 2,3,3,3-TETRAFLUORO-1-PHENYL- 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)C(C(F)(F)F)F

Technology Process of 2,3,3,3-Tetrafluoro-1-phenylpropan-1-one

There total 10 articles about 2,3,3,3-Tetrafluoro-1-phenylpropan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(perfluoroprop-1-enyl)benzene (41424-70-8,41500-48-5,345-79-9) → phenyl 1,2,2,2,-tetrafluoroethyl ketone (2267-65-4)

Guidance literature:

With sulfuric acid;

DOI:10.1007/BF00942891

Reference yield:

(Z)-1-ethoxy-1-phenyltetrafluoropropene → phenyl 1,2,2,2,-tetrafluoroethyl ketone (2267-65-4)

Guidance literature:

With hydrogenchloride; at 20 ℃; for 18h; Yield given;

DOI:10.1016/S0022-1139(00)81242-7

Reference yield:

(E/Z)-1-phenyl-2,3,3,3-tetrafluoro-1-trimethylsiloxypropene → phenyl 1,2,2,2,-tetrafluoroethyl ketone (2267-65-4)

Guidance literature:

With hydrogenchloride; at 20 ℃; for 5h;

DOI:10.1016/j.jfluchem.2007.12.003

upstream raw materials:

(perfluoroprop-1-enyl)benzene

benzoyl fluoride

1,1,2-trifluoroethylene

2,3,3,3-tetrafluoropropionitrile

Downstream raw materials:

ethyl 2-fluoro-3-oxo-3-phenylpropionate

(Z)-1-phenyl-3,3,3-trifluoro-1-trimethylsiloxypropene

α,β,β,β-Tetrafluor-3-nitro-propiophenon

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