(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

Base Information

Chemical Name:(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate
CAS No.:1418466-30-4
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:

Synonyms:(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

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Chemical Property of (2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

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Technology Process of (2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

There total 3 articles about (2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1222011-04-2
methyl cis-3-[{(1'R)-phenylethylaziridin}-(2R)-yl]acrylate

: 1418466-30-4
(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

Guidance literature:: With hydroquinidine 1 4-phthalazinediyl diether; methanesulfonamide; In water; butan-1-ol; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2012.11.087

Reference yield:

: 1222011-04-2
methyl cis-3-[{(1'R)-phenylethylaziridin}-(2R)-yl]acrylate

: 1418466-68-8
C₁₄H₁₉NO₄

: 1418466-30-4
(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

Guidance literature:: With hydroquinidine 1 4-phthalazinediyl diether; methanesulfonamide; In water; butan-1-ol; at 20 ℃; for 24h; Overall yield = 70 %;
DOI:10.1016/j.tetlet.2012.11.087

Reference yield:

: [1'(R)-α-methylbenzyl]aziridine-2(R)-carboxaldehyde

: 1418466-68-8
C₁₄H₁₉NO₄

: 1418466-30-4
(2S,3S)-methyl 2,3-dihydroxy-3-((R)-1-((R)-1-phenylethyl)aziridin-2-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0 °C

2: hydroquinidine 1 4-phthalazinediyl diether; methanesulfonamide / water; butan-1-ol / 24 h / 20 °C

With hydroquinidine 1 4-phthalazinediyl diether; methanesulfonamide; In methanol; water; butan-1-ol; 1: |Wittig Olefination;
DOI:10.1016/j.tetlet.2012.11.087