2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Base Information

Chemical Name:2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine
CAS No.:84694-28-0
Molecular Formula:C₂₈H₄₁NO₂Si
Molecular Weight:451.725
Hs Code.:

2-<o-<1-(trimethylsilyl)hept-6-enyl>phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Synonyms:2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

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Chemical Property of 2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Chemical Property:

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Technology Process of 2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

There total 7 articles about 2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18922-04-8
6-iodohex-1-ene

: 84694-28-0
2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 1.) n-BuLi / 1.) ether, hexane, 0 deg C, 30 min, 2.) HMPA, RT, overnight

2: 90 percent / acetonitrile / 7 h / 40 - 50 °C

3: 1.) NaBH₄, Et₃N, 2.) 5percent HCl / 1.) EtOH, -78 deg C, 1 min, 2.) -78 deg C -> RT, 3 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; triethylamine; In acetonitrile;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-18-8
2-{o-[(trimethylsilyl)methyl]phenyl}-4,4-dimethyloxazoline

: 84694-28-0
2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 1.) n-BuLi / 1.) ether, hexane, 0 deg C, 30 min, 2.) HMPA, RT, overnight

2: 90 percent / acetonitrile / 7 h / 40 - 50 °C

3: 1.) NaBH₄, Et₃N, 2.) 5percent HCl / 1.) EtOH, -78 deg C, 1 min, 2.) -78 deg C -> RT, 3 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; triethylamine; In acetonitrile;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-19-9
2-phenyl>-4,4-dimethyloxazoline

: 84694-28-0
2-phenyl>-3-methyl-4(S)-methoxymethyl-5(S)-phenyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / acetonitrile / 7 h / 40 - 50 °C

2: 1.) NaBH₄, Et₃N, 2.) 5percent HCl / 1.) EtOH, -78 deg C, 1 min, 2.) -78 deg C -> RT, 3 h

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In acetonitrile;
DOI:10.1021/ja00344a028