2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

Base Information

Chemical Name:2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene
CAS No.:366002-40-6
Molecular Formula:C₁₃H₁₃F₅O₆S
Molecular Weight:392.301
Hs Code.:

Synonyms:2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

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Chemical Property of 2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

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Technology Process of 2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

There total 3 articles about 2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 109586-39-2
4-iodophenyl trifluoromethanesulfonate

: 170941-63-6
2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-(tributylstannyl)ethene

: 366002-40-6
2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

Guidance literature:: With copper(l) iodide; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 50 ℃; for 16h;
DOI:10.1021/ol010135p

Reference yield: 65.0%

: potassium 2,2-difluoro-1-(2-methoxy-ethoxymethoxy)ethenyltrifluoroborate

: 109586-39-2
4-iodophenyl trifluoromethanesulfonate

: 366002-40-6
2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In propan-1-ol; at 90 ℃; for 21h;
DOI:10.1039/c1ob06372c

Reference yield: 25.0%

: 2,2-difluoro-1-((2-methoxy)ethoxymethoxy)ethenylzinc chloride

: 109586-39-2
4-iodophenyl trifluoromethanesulfonate

: 366002-40-6
2,2-difluoro-1-(2-methoxy-ethoxymethoxy)-1-[4-(trifluoromethanesulfonyloxy)phenyl]ethene

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 65 ℃; for 16h;
DOI:10.1039/c1ob06372c