1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

Base Information

Chemical Name:1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol
CAS No.:932378-53-5
Molecular Formula:C₃₉H₅₃NO₈S
Molecular Weight:695.918
Hs Code.:

Synonyms:1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

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Chemical Property of 1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

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Technology Process of 1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

There total 15 articles about 1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 932378-50-2
1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-3-(p-toluenesulfonyl)-sn-glycerol

: 932378-53-5
1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo062352f

Reference yield:

: 41274-09-3
(R)-3-tosyloxy-1,2-propanediol

: 932378-53-5
1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / DMAP / CH₂Cl₂ / 96 h / 20 °C

2: 89 percent / PPTS / CH₂Cl₂ / 24 h / 20 °C

With dmap; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1021/jo062352f

Reference yield:

: 23788-74-1,7305-59-1
(R)-2,2-dimethyl-1,3-dioxolane-4-ylmethyl p-toluenesulfonate

: 932378-53-5
1-(12'-N-[2''-naphthylacetyl]aminolauroyl)-2-(tetrahydropyran-2-yl)-3-(p-toluenesulfonyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / HCl / methanol / 0.5 h / 20 °C

2: 58 percent / DMAP / CH₂Cl₂ / 96 h / 20 °C

3: 89 percent / PPTS / CH₂Cl₂ / 24 h / 20 °C

With hydrogenchloride; dmap; pyridinium p-toluenesulfonate; In methanol; dichloromethane;
DOI:10.1021/jo062352f