(3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Base Information

Chemical Name:(3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester
CAS No.:854938-43-5
Molecular Formula:C₃₃H₄₁NO₅S₂
Molecular Weight:595.824
Hs Code.:

Synonyms:(3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Suppliers and Price of (3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

There total 2 articles about (3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 854938-42-4
(S)-N-tertiobutoxycarbonylamino-S-trityl-cysteine methyl ester

: neopentyl diethoxyphosphorylmethanesulfonate

: 854938-43-5
(3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Guidance literature:: neopentyl diethoxyphosphorylmethanesulfonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(S)-N-tertiobutoxycarbonylamino-S-trityl-cysteine methyl ester; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; toluene; at -78 ℃;
DOI:10.1002/jlcr.888

Reference yield:

: N-(tert-butoxycarbonyl)-S-trityl-D-cysteine

: 854938-43-5
(3S)-3-tertiobutoxycarbonylamino-4-tritylsulfanyl-but-1-ene-1-sulfonic acid 2,2-dimethylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether; methanol / 6 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 2.4 g / diisobutyl aluminium hydride / tetrahydrofuran; hexane; toluene / -78 °C

With n-butyllithium; In tetrahydrofuran; methanol; diethyl ether; hexane;
DOI:10.1002/jlcr.888