(E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

Base Information

Chemical Name:(E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide
CAS No.:1361391-55-0
Molecular Formula:C₃₄H₂₆N₂O₄S₂
Molecular Weight:590.723
Hs Code.:

Synonyms:(E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

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Technology Process of (E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

There total 1 articles about (E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-14-2
2-bromonaphthalen-1-amine

: 1361391-55-0
(E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 12 h / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 4 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ol300166q

Reference yield: 77.0%

: 1361391-55-0
(E)-N,N'-[2,2'-(ethene-1,2-diyl)bis(naphthalene-2,1-diyl)]dibenzenesulfonamide

: 7,14-bis(phenylsulfonyl)-6b,7,13b,14-tetrahydrobenzo[g]benz[6,7]indolo[3,2-b]indole

Guidance literature:: With [bis(acetoxy)iodo]benzene; tetrabutyl-ammonium chloride; In N,N-dimethyl-formamide; at 25 ℃; for 6h; diastereoselective reaction;
DOI:10.1021/ol300166q