1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Base Information

Chemical Name:1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine
CAS No.:77563-31-6
Molecular Formula:C₂₅H₃₂N₄O₂S
Molecular Weight:452.621
Hs Code.:

Synonyms:1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Chemical Property:

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Technology Process of 1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

There total 4 articles about 1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.5%

: 5407-56-7
2-isopropoxybenzo[d]thiazole-6-amine

: 77563-21-4
1-(2-bromopropionyl)-4-phenethylpiperazine

: 77563-31-6
1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Guidance literature:: With potassium carbonate; In ethanol; for 5h; Heating;
DOI:10.1248/cpb.28.3315

Reference yield:

: 5321-49-3
4-(phenethyl)piperazine

: 77563-31-6
1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Guidance literature:: Multi-step reaction with 2 steps

1: 16 g / benzene / 2 h / 5 °C

2: 52.5 percent / K₂CO₃ / ethanol / 5 h / Heating

With potassium carbonate; In ethanol; benzene;
DOI:10.1248/cpb.28.3315

Reference yield:

: 2407-11-6
2-chloro-6-nitrobenzothiazole

: 77563-31-6
1-<2-(2-isopropoxy-benzothiazolyl-(6))-aminopropionyl>-4-phenethylpiperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 51.2 percent / sodium / 5 h / Heating

2: 33.9 percent / iron, 50percent aq. acetic acid / ethanol / 2 h / Heating

3: 52.5 percent / K₂CO₃ / ethanol / 5 h / Heating

With sodium; iron; potassium carbonate; acetic acid; In ethanol;
DOI:10.1248/cpb.28.3315