(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

Base Information

Chemical Name:(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride
CAS No.:1431371-94-6
Molecular Formula:C₂₆H₂₉NO₃*ClH
Molecular Weight:439.982
Hs Code.:

Synonyms:(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

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Chemical Property of (2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

Chemical Property:

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Technology Process of (2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

There total 4 articles about (2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1431371-92-4
C₃₁H₃₇NO₅

: 1431371-94-6
(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

Guidance literature:: With methanol; acetyl chloride;
DOI:10.1016/j.tetlet.2013.02.115

Reference yield:

: 84366-59-6
(2S,3R,4R)-2,3,5-tri-O-benzyl-pentane-1,4-diol

: 1431371-94-6
(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; iodine / 36 h / -30 °C

2: sodium azide / N,N-dimethyl-formamide / 3 h / 50 °C

3: triphenylphosphine; water / tetrahydrofuran

4: sodium hydroxide

5: acetyl chloride; methanol

With methanol; sodium azide; water; iodine; acetyl chloride; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.02.115

Reference yield:

: 1431371-87-7
(2S,3S,4R)-1,3,4-tribenzyloxy-2,5-diiodopentane

: 1431371-94-6
(2R,3R,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)pyrrolidine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 3 h / 50 °C

2: triphenylphosphine; water / tetrahydrofuran

3: sodium hydroxide

4: acetyl chloride; methanol

With methanol; sodium azide; water; acetyl chloride; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.02.115