(CH₃C₅H₄)(C₅H₅)3V₄S₄

Base Information

• Chemical Name: (CH₃C₅H₄)(C₅H₅)3V₄S₄
• CAS No.: 111237-38-8
• Molecular Formula: C₂₁H₂₂S₄V₄
• Molecular Weight: 606.436
• Mol file: 111237-38-8.mol

Synonyms:(CH₃C₅H₄)(C₅H₅)3V₄S₄

Chemical Property of (CH₃C₅H₄)(C₅H₅)3V₄S₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (CH₃C₅H₄)(C₅H₅)3V₄S₄

There total 1 articles about (CH₃C₅H₄)(C₅H₅)3V₄S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2(C5H5)(1-)*V2S4(2+) (111266-88-7) + 2(CH3C5H4)(1-)*V2S4(2+) (87174-39-8) + tributylphosphine (998-40-3) → Cp'4V4S4 + (CH3C5H4)(C5H5)3V4S4 (111237-38-8) + (CH3C5H4)3(C5H5)V4S4 (111266-89-8) + (CH3C5H4)2(C5H5)2V4S4 (111237-37-7) + tri-n-butylphosphine sulfide (3084-50-2)

Guidance literature:

In dichloromethane; a soln. of (Cp)2V2S4 in CH2Cl2 is added to a soln. of (CH3C5H4)2V2S4 in CH2Cl2; a soln. of (n-Bu)3P is added, the resulting mixt. stirred for 1 h at room temp.; 1 further product formed; solvent removed in vac., residue extd. with hexane; ext. concd. to give a black microcrystalline solid; products not further sepd.;

DOI:10.1021/ja00209a023

upstream raw materials:

2(C₅H₅)^(1-)*V₂S₄⁽²⁺⁾

2(CH₃C₅H₄)^(1-)*V₂S₄⁽²⁺⁾

tributylphosphine