C₃₂H₄₀ClF₃O₁₀SSi

Base Information

Chemical Name:C₃₂H₄₀ClF₃O₁₀SSi
CAS No.:1332271-27-8
Molecular Formula:C₃₂H₄₀ClF₃O₁₀SSi
Molecular Weight:737.263
Hs Code.:

C<sub>32</sub>H<sub>40</sub>ClF<sub>3</sub>O<sub>10</sub>SSi

Synonyms:C₃₂H₄₀ClF₃O₁₀SSi

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Chemical Property of C₃₂H₄₀ClF₃O₁₀SSi

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Technology Process of C₃₂H₄₀ClF₃O₁₀SSi

There total 5 articles about C₃₂H₄₀ClF₃O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332271-64-3
C₃₂H₄₂ClF₃O₁₀SSi

: 1332271-27-8
C₃₂H₄₀ClF₃O₁₀SSi

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: C₃₁H₄₅ClO₇Si

: 1332271-27-8
C₃₂H₄₀ClF₃O₁₀SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

With pyridine; tetrapropylammonium perruthennate; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; pyridine hydrogenfluoride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1332271-63-2
C₃₁H₄₃ClO₇Si

: 1332271-27-8
C₃₂H₄₀ClF₃O₁₀SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

With pyridine; tetrapropylammonium perruthennate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.04.094