N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

Base Information

Chemical Name:N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester
CAS No.:93471-96-6
Molecular Formula:C₁₈H₂₃NS
Molecular Weight:285.453
Hs Code.:

Synonyms:N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

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Chemical Property of N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

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Technology Process of N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

There total 1 articles about N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73670-87-8
(E)-hexa-3,5-dien-1-ol

: N-(2,6-Dimethylphenyl)-α-methacrylthioamide

: 93471-96-6
N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

Guidance literature:: With tributylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at -78 - 0 ℃; Yield given;
DOI:10.1016/S0040-4039(01)91081-0

Reference yield: 68.0%

: 93471-96-6
N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

: 93472-05-0,93472-06-1
(2,6-Dimethyl-phenyl)-[(4aS,8aR)-8a-methyl-3,4,4a,7,8,8a-hexahydro-isothiochromen-(1Z)-ylidene]-amine

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; for 80h; Ambient temperature;
DOI:10.1016/S0040-4039(01)91081-0

Reference yield:

: 93471-96-6
N-(2,6-Dimethyl-phenyl)-2-methyl-thioacrylimidic acid (E)-hexa-3,5-dienyl ester

: 93472-05-0,93472-06-1
(2,6-Dimethyl-phenyl)-[8a-methyl-3,4,4a,7,8,8a-hexahydro-isothiochromen-(1Z)-ylidene]-amine

Guidance literature:: In various solvent(s); at 160 ℃; for 13h; Yield given; trace of hydroquinone monomethyl ether;
DOI:10.1016/S0040-4039(01)91081-0