5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

Base Information

Chemical Name:5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine
CAS No.:350237-68-2
Molecular Formula:C₃₇H₃₈N₄O₈
Molecular Weight:666.731
Hs Code.:

5'-O-(4,4'-dimethoxytrityl)-N<sub>1</sub>-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

Synonyms:5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

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Technology Process of 5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

There total 5 articles about 5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 350237-69-3
N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

: 350237-68-2
5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

Guidance literature:: With pyridine; at 20 ℃; for 120h;
DOI:10.1021/tx010025r

Reference yield:

: 890-38-0
2-deoxyinosine

: 350237-68-2
5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 48 h / 20 °C

2: 80 percent / pyridine / 120 h / 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/tx010025r

Reference yield:

: 64623-51-4
4-acetoxy-3-bromo-1-butene

: 350237-68-2
5'-O-(4,4'-dimethoxytrityl)-N₁-(1-acetoxy-3-buten-2-yl)-2'-deoxyinosine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 48 h / 20 °C

2: 80 percent / pyridine / 120 h / 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/tx010025r