C₂₇H₃₃N₃O₇S

Base Information

Chemical Name:C₂₇H₃₃N₃O₇S
CAS No.:868287-30-3
Molecular Formula:C₂₇H₃₃N₃O₇S
Molecular Weight:543.641
Hs Code.:

C<sub>27</sub>H<sub>33</sub>N<sub>3</sub>O<sub>7</sub>S

Synonyms:C₂₇H₃₃N₃O₇S

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Chemical Property of C₂₇H₃₃N₃O₇S

Chemical Property:

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Technology Process of C₂₇H₃₃N₃O₇S

There total 6 articles about C₂₇H₃₃N₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₅N₃O₈S

: 868287-30-3
C₂₇H₃₃N₃O₇S

Guidance literature:: With Burgess Reagent; In 1,2-dichloro-ethane; at 80 ℃; for 0.25h; Microwave;

Reference yield:

: 99-27-4
dimethyl 5-aminoisophthalate

: 868287-30-3
C₂₇H₃₃N₃O₇S

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dichloromethane / 4 h / 0 - 20 °C

2: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h

3: methanol; sodium hydroxide / tetrahydrofuran / 8 h / 0 - 20 °C

4: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 50 h / 20 °C

5: pyridine-SO₃ complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3.5 h / 20 °C

6: Burgess Reagent / 1,2-dichloro-ethane / 0.25 h / 80 °C / Microwave

With pyridine; methanol; sodium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; pyridine-SO₃ complex; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;

Reference yield:

: 868287-28-9
C₂₇H₃₇N₃O₈S

: 868287-30-3
C₂₇H₃₃N₃O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine-SO₃ complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3.5 h / 20 °C

2: Burgess Reagent / 1,2-dichloro-ethane / 0.25 h / 80 °C / Microwave

With Burgess Reagent; pyridine-SO₃ complex; triethylamine; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;