dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

Base Information

Chemical Name:dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate
CAS No.:1416338-26-5
Molecular Formula:C₂₄H₂₇N₂O₆P
Molecular Weight:470.462
Hs Code.:

Synonyms:dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

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Chemical Property of dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

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Technology Process of dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

There total 2 articles about dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 95-53-4
o-toluidine

: (diazo(4-methylphenyl)methyl)dimethyl phosphonate

: 1416338-26-5
dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

: dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

: 1416338-39-0
dimethyl 1-(o-toluidino)-2-hydroxy-2-(3-nitrophenyl)-1-phenylethylphosphonate

Guidance literature:: With C₂₆H₃₈NO₄Rh₂; In dichloromethane; at 40 ℃; enantioselective reaction;
DOI:10.1002/anie.201206551 DOI:10.1002/anie.201206551

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 95-53-4
o-toluidine

: (diazo(4-methylphenyl)methyl)dimethyl phosphonate

: 1416338-26-5
dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

: dimethyl 1-(o-toluidino)-2-hydroxy-2-(4-nitrophenyl)-1-p-tolylethyl-phosphonate

Guidance literature:: With C₂₆H₃₈NO₄Rh₂; In dichloromethane; at 40 ℃; Overall yield = 78 %; enantioselective reaction;
DOI:10.1002/anie.201206551 DOI:10.1002/anie.201206551