4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

Base Information

Chemical Name:4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine
CAS No.:1268250-86-7
Molecular Formula:C₅₈H₃₈N₄
Molecular Weight:790.967
Hs Code.:

Synonyms:4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

There total 6 articles about 4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1268250-86-7
4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

Guidance literature:: With palladium diacetate; XPhos; In tetrahydrofuran; at 60 ℃; for 0.166667h; Inert atmosphere;

With potassium carbonate; In tetrahydrofuran; water; at 75 ℃; for 10h; Inert atmosphere;

Reference yield:

: 1073062-76-6
2,4-bis({[1,1'-biphenyl]-3-yl})-6-(3,5-dibromophenyl)-1,3,5-triazine

: 68572-87-2
9-phenanthrenylboronic acid

: 1268250-86-7
4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 3 h / 60 °C / Inert atmosphere

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 4 h / 60 °C / Inert atmosphere

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene;

Reference yield:

: 170230-27-0
(4-(pyridin-2-yl)phenyl)boronic acid

: C₄₇H₃₀BrN₃

: 1268250-86-7
4,6-bis(biphenyl-3-yl)-2-[5-(9-phenathryl)-4'-(2-pyridyl)biphenyl-3-yl]-1,3,5-triazine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 60 ℃; for 4h; Inert atmosphere;