4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

Base Information

Chemical Name:4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate
CAS No.:1615654-51-7
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

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Chemical Property of 4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

Chemical Property:

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Technology Process of 4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

There total 6 articles about 4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1615654-44-8
tert-Butyl 3-[4-(2-hydroxyethyl)phenoxyl]-3-phenylpropyl(methyl)carbamate

: 108-24-7
acetic anhydride

: 1615654-51-7
4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 19h;

Reference yield:

: 1615654-43-7
methyl 2-[4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy] phenyl]acetate

: 1615654-51-7
4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: acetic anhydride; triethylamine / ethyl acetate

With acetic anhydride; triethylamine; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 1615654-51-7
4-[3-[tert-butoxycarbonyl(methyl)amino]-1-phenylpropoxy]phenethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / ethyl acetate; toluene; hexane

2: tetrahydrofuran

3: acetic anhydride; triethylamine / ethyl acetate

With acetic anhydride; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; ethyl acetate; toluene;