Technology Process of C50H40O10
There total 1 articles about C50H40O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
dichloromethane;
for 20h;
Ambient temperature;
DOI:10.1039/a700841d
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
for 48h;
Ambient temperature;
DOI:10.1039/a700841d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / H2 / 5percent Pd/C / tetrahydrofuran / 48 h / Ambient temperature
2: 84.1 percent / 4-N,N-dimethylaminopyridinium toluene-p-sulfonate, DCC / dimethylformamide / 24 h / Ambient temperature
3: 82.5 percent / NaI, AlCl3 / acetonitrile / 12 h / Heating
With
aluminium trichloride; hydrogen; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; sodium iodide;
palladium on activated charcoal;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/a700841d