2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione

Base Information

• Chemical Name: 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione
• CAS No.: 93031-41-5
• Molecular Formula: C₂₇H₁₈BrN₅S
• Molecular Weight: 524.443

Synonyms:2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione

Chemical Property of 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione

Chemical Property:

Purity/Quality:

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Technology Process of 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione

There total 3 articles about 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(4-Bromo-phenyl)-3-(3-cyano-5,7-diphenyl-pyrazolo[1,5-a]pyridin-2-yl)-thiourea (93031-38-0) → 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione (93031-41-5)

Guidance literature:

With triethylamine; In pyridine; for 10h; Heating;

DOI:10.1002/jhet.5570210311

Reference yield:

2-amino-3-cyano-5,7-diphenylpyrazolo<1,5-a>pyridine (80355-94-8) → 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione (93031-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / triethylamine / dimethylformamide / 18 h / Ambient temperature

2: 85 percent / triethylamine / pyridine / 10 h / Heating

With triethylamine; In pyridine; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570210311

Reference yield:

4-Bromophenyl isothiocyanate (1985-12-2) → 2-(4-Bromo-phenylamino)-6,8-diphenyl-3H-1,3,8a,9-tetraaza-fluorene-4-thione (93031-41-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / triethylamine / dimethylformamide / 18 h / Ambient temperature

2: 85 percent / triethylamine / pyridine / 10 h / Heating

With triethylamine; In pyridine; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570210311

upstream raw materials:

1-(4-Bromo-phenyl)-3-(3-cyano-5,7-diphenyl-pyrazolo[1,5-a]pyridin-2-yl)-thiourea

2-amino-3-cyano-5,7-diphenylpyrazolo<1,5-a>pyridine

4-Bromophenyl isothiocyanate

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