tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

Base Information

Chemical Name:tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester
CAS No.:1236357-27-9
Molecular Formula:C₂₃H₂₉N₅O₄
Molecular Weight:439.514
Hs Code.:

Synonyms:tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

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Chemical Property of tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

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Technology Process of tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

There total 3 articles about tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimido[5,4-f][1,4]oxazepin-6(5H)-yl)-phenyl}-5,6-dihydroxypyridine-1(2H)-carboxylic ester

: 1236357-27-9
tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; sodium acetate; In methanol; at 20 ℃; for 12h;

Reference yield:

: 1338326-89-8
4-amino-6-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-7,8-dihydropyrimido[5,4-f][1,4]oxazepin-5(6H)-one

: 1236357-27-9
tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / tetrahydrofuran; water / 12 h / 80 °C

2: palladium 10% on activated carbon; hydrogen; sodium acetate / methanol / 12 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; sodium acetate; sodium carbonate; In tetrahydrofuran; methanol; water;

Reference yield:

: 138647-49-1
4-Trifluoromethanesulfonyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester

: 1236357-27-9
tertiary butyl 4-{4-(4-amino-5-oxo-7,8-dihydropyrimidine[5,4-f][1,4] oxazepin-6(5H)yl)-phenyl}pyridine-1-carboxylic ester

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / tetrahydrofuran; water / 12 h / 80 °C

2: palladium 10% on activated carbon; hydrogen; sodium acetate / methanol / 12 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; sodium acetate; sodium carbonate; In tetrahydrofuran; methanol; water;