[1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine

Base Information

• Chemical Name: [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine
• CAS No.: 387850-89-7
• Molecular Formula: C₂₄H₂₅NO₅
• Molecular Weight: 407.466
• Mol file: 387850-89-7.mol

Synonyms:[1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine

Chemical Property of [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine

There total 1 articles about [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-Trimethoxyaniline (24313-88-0) + 3-benzyloxy-4-methoxybenzaldehyde (6346-05-0) → [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine (387850-89-7)

Guidance literature:

With acetic acid; In ethanol; for 2h; Heating;

DOI:10.1021/jm010523x

Reference yield:

[1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine (387850-89-7) → 2-methoxy-5-[3-(3,4,5-trimethoxy-phenyl)-3H-imidazol-4-yl]-phenol

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / methanol; 1,2-dimethoxy-ethane / Heating

2: H₂ / 5percent Pd/C / ethyl acetate / 20 °C

With hydrogen; potassium carbonate; 5percent Pd/C; In methanol; 1,2-dimethoxyethane; ethyl acetate;

DOI:10.1021/jm010523x

Reference yield:

[(p-methylphenyl)sulfonylmethyl]isonitrile (38622-91-2,36635-61-7) + [1-(3-Benzyloxy-4-methoxy-phenyl)-meth-(Z)-ylidene]-(3,4,5-trimethoxy-phenyl)-amine (387850-89-7) → 5-(3-benzyloxy-4-methoxy-phenyl)-1-(3,4,5-trimethoxy-phenyl)-1H-imidazole (424834-27-5)

Guidance literature:

With potassium carbonate; In methanol; 1,2-dimethoxyethane; Heating;

DOI:10.1021/jm010523x

upstream raw materials:

3,4,5-Trimethoxyaniline

3-benzyloxy-4-methoxybenzaldehyde

Downstream raw materials:

5-(3-benzyloxy-4-methoxy-phenyl)-1-(3,4,5-trimethoxy-phenyl)-1H-imidazole