ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

Base Information

Chemical Name:ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate
CAS No.:1357927-41-3
Molecular Formula:C₂₂H₂₃N₃O₂
Molecular Weight:361.444
Hs Code.:

Synonyms:ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

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Chemical Property of ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

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Technology Process of ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

There total 4 articles about ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 289037-49-6
1-(cyclopropylmethyl)-5-amino-1H-indole

: 5499-31-0
thiobenzoyl-carbamic acid ethyl ester

: 1357927-41-3
ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

Guidance literature:: In ethanol; Reflux;
DOI:10.1016/j.ejmech.2011.12.026

Reference yield:

: 1-(cyclopropylmethyl)-5-nitro-1H-indole

: 1357927-41-3
ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / 30 - 40 °C

2: ethanol / Reflux

With palladium 10% on activated carbon; hydrogen; In ethanol;
DOI:10.1016/j.ejmech.2011.12.026

Reference yield:

: 6146-52-7
5-nitroindole

: 1357927-41-3
ethyl (1-(cyclopropylmethyl)-1H-indol-5-ylamino)(phenyl)methylenecarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / toluene / Reflux

2: palladium 10% on activated carbon; hydrogen / 30 - 40 °C

3: ethanol / Reflux

With palladium 10% on activated carbon; hydrogen; sodium hydride; In ethanol; toluene;
DOI:10.1016/j.ejmech.2011.12.026