methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

Base Information

Chemical Name:methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1
CAS No.:106689-77-4
Molecular Formula:C₁₈H₁₄ClN₃O
Molecular Weight:323.782
Hs Code.:

Synonyms:methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

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Chemical Property of methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

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Technology Process of methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

There total 1 articles about methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-3-(1-Benzyl-4-chloro-1H-pyrrolo[3,2-c]pyridin-2-yl)-but-2-enoyl azide

: 106689-77-4
methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

Guidance literature:: With tributyl-amine; In diphenylether; at 230 - 240 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4020(01)90611-8

Reference yield: 92.0%

: 106689-77-4
methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

: 106689-79-6
methyl-4 benzyl-5-2H-5H-pyrido<3',4':4,5>pyrrolo<3,2-c>pyridone-1

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; for 2h; under 760 Torr; Ambient temperature;
DOI:10.1016/S0040-4020(01)90611-8

Reference yield:

: 106689-77-4
methyl-4 benzyl-5 chloro-9-2H-5H-pyrido<3'4':4,5>pyrrolo<3,2-c>pyridone-1

: 106689-85-4
(γ-diethylamino)propylamino-1 methyl-4 benzyl-5-5H-pyrido<3',4':4,5>pyrrolo<3,2-c>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / hydrogen, triethylamine / 10percent Pd/C / ethanol / 2 h / 760 Torr / Ambient temperature

2: 79.9 percent / phenylphosphonic dichloride / 2 h / Heating

3: 72 h / 170 °C

With P,P-dichlorophenylphosphine oxide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)90611-8