2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

Base Information

Chemical Name:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate
CAS No.:1345985-91-2
Molecular Formula:C₂₈H₃₃NO₅S
Molecular Weight:495.64
Hs Code.:

Synonyms:2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

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Chemical Property of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

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Technology Process of 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

There total 8 articles about 2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2905-27-3
3,5-dimethyl-benzenesulfonyl chloride

: 215391-96-1
rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol

: 1345985-91-2
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

Guidance literature:: rac-2-(N-tert-Butoxycarbonyl-N-benzylamino)-1-phenylethanol; With potassium hydroxide; In tetrahydrofuran; for 0.25h;

3,5-dimethyl-benzenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 96-09-3
styrene oxide

: 1345985-91-2
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: activated silica / 24 h / Inert atmosphere

2: triethylamine / methanol / 0.5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 51096-49-2,91579-12-3,107171-75-5,27159-30-4
2-benzylamino-1-phenyl-ethanol

: 1345985-91-2
2-(benzyl(tert-butoxycarbonyl)amino)-1-phenylethyl 3,5-dimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 0.5 h / Reflux

2: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078