C₄₂H₆₀N₄O₈

Base Information

Chemical Name:C₄₂H₆₀N₄O₈
CAS No.:1313405-24-1
Molecular Formula:C₄₂H₆₀N₄O₈
Molecular Weight:748.96
Hs Code.:

C<sub>42</sub>H<sub>60</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:C₄₂H₆₀N₄O₈

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Chemical Property of C₄₂H₆₀N₄O₈

Chemical Property:

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Technology Process of C₄₂H₆₀N₄O₈

There total 7 articles about C₄₂H₆₀N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313405-21-8
C₂₀H₃₀N₂O₄

: 1313405-22-9
C₂₂H₃₂N₂O₅

: 1313405-24-1
C₄₂H₆₀N₄O₈

Guidance literature:: C₂₂H₃₂N₂O₅; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

C₂₀H₃₀N₂O₄; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol201282d

Reference yield:

: 13736-58-8
2-(octyloxy)-5-nitro-benzoic acid

: 1313405-24-1
C₄₂H₆₀N₄O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: hydrogenchloride; iron / methanol; water / 6 h / Reflux; Inert atmosphere

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.2: 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; iron; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/ol201282d

Reference yield:

: 267897-49-4
2-octyloxy-5-nitro-benzoic acid methyl ester

: 1313405-24-1
C₄₂H₆₀N₄O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; potassium hydroxide / 4 h / 60 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: hydrogenchloride; iron / methanol; water / 6 h / Reflux; Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.2: 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; water; iron; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/ol201282d