2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate

Base Information

• Chemical Name: 2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate
• CAS No.: 1177502-53-2
• Molecular Formula: C₃₂H₄₈O₇S
• Molecular Weight: 576.795

Synonyms:2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate

Chemical Property of 2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate

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Technology Process of 2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate

There total 1 articles about 2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethanol (864876-19-7) + p-toluenesulfonyl chloride (98-59-9) → 2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate (1177502-53-2)

Guidance literature:

2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethanol; With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 1h;

p-toluenesulfonyl chloride; In tetrahydrofuran; water; at 0 - 20 ℃;

DOI:10.1039/b902848j

Reference yield: 99.0%

2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate (1177502-53-2) + methyl 4-hydroxylbenzoate (99-76-3,156291-94-0) → methyl 4-{2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethoxy}benzoate (1177502-57-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;

DOI:10.1039/b902848j

Reference yield: 75.0%

2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethyl tosylate (1177502-53-2) + methyl galloate (99-24-1) → methyl 3,4,5-tris{2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethoxy}benzoate (1177502-55-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 10h; Inert atmosphere;

DOI:10.1039/b902848j

upstream raw materials:

2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethanol

p-toluenesulfonyl chloride

Downstream raw materials:

methyl 3,4,5-tris{2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethoxy}benzoate

methyl 4-{2-[2-(2-{2-[4-(4-trans-pentylcyclohexyl)phenoxy]ethoxy}ethoxy)ethoxy]ethoxy}benzoate

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