C₃₈H₄₇N₃O₁₁Si

Base Information

Chemical Name:C₃₈H₄₇N₃O₁₁Si
CAS No.:1415724-90-1
Molecular Formula:C₃₈H₄₇N₃O₁₁Si
Molecular Weight:749.89
Hs Code.:

C<sub>38</sub>H<sub>47</sub>N<sub>3</sub>O<sub>11</sub>Si

Synonyms:C₃₈H₄₇N₃O₁₁Si

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Chemical Property of C₃₈H₄₇N₃O₁₁Si

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Technology Process of C₃₈H₄₇N₃O₁₁Si

There total 6 articles about C₃₈H₄₇N₃O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: C₄₂H₅₁N₃O₁₃Si

: 1415724-90-1
C₃₈H₄₇N₃O₁₁Si

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at 0 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol303122w

Reference yield:

: C₂₂H₂₄Cl₃NO₆S

: 1415724-90-1
C₃₈H₄₇N₃O₁₁Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap / pyridine / 12 h / 20 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 1 h / -60 °C / Molecular sieve; Inert atmosphere

3.1: zinc; acetic acid / acetonitrile / 1 h / 20 °C / Inert atmosphere

4.1: triflic azide; pyridine; copper(II) sulfate; triethylamine / 3 h / 0 °C

5.1: sodium methylate; methanol / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere

With pyridine; methanol; dmap; triflic azide; sodium methylate; copper(II) sulfate; acetic acid; triethylamine; zinc; In tetrahydrofuran; pyridine; dichloromethane; acetonitrile;
DOI:10.1021/ol303122w

Reference yield:

: 1415724-84-3
C₂₆H₂₈Cl₃NO₈S

: 1415724-90-1
C₃₈H₄₇N₃O₁₁Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 1 h / -60 °C / Molecular sieve; Inert atmosphere

2.1: zinc; acetic acid / acetonitrile / 1 h / 20 °C / Inert atmosphere

3.1: triflic azide; pyridine; copper(II) sulfate; triethylamine / 3 h / 0 °C

4.1: sodium methylate; methanol / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere

With pyridine; methanol; triflic azide; sodium methylate; copper(II) sulfate; acetic acid; triethylamine; zinc; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol303122w