C₁₈H₂₂O₇

Base Information

Chemical Name:C₁₈H₂₂O₇
CAS No.:934747-55-4
Molecular Formula:C₁₈H₂₂O₇
Molecular Weight:350.368
Hs Code.:

C<sub>18</sub>H<sub>22</sub>O<sub>7</sub>

Synonyms:C₁₈H₂₂O₇

Suppliers and Price of C₁₈H₂₂O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₂₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₂₂O₇

There total 1 articles about C₁₈H₂₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 934747-54-3
C₁₈H₂₂O₇

: 934747-55-4
C₁₈H₂₂O₇

Guidance literature:: With di(rhodium)tetracarbonyl dichloride; In tetrahydrofuran; at 25 ℃; Further Variations:; Reagents; Solvents; Temperatures; Product distribution;
DOI:10.1016/j.tetlet.2007.01.102

Reference yield: 80.0%

: 934747-55-4
C₁₈H₂₂O₇

: 934747-56-5
C₁₇H₂₄O₆

Guidance literature:: With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; ethanol; at -78 ℃;
DOI:10.1016/j.tetlet.2007.01.102

Reference yield:

: 934747-55-4
C₁₈H₂₂O₇

: C₄₈H₆₄O₁₁Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: 80 percent / KBH(s-Bu)3 / tetrahydrofuran; ethanol / -78 °C

2.1: n-Bu₃P / tetrahydrofuran / 20 °C

3.1: H₂O₂ / tetrahydrofuran; H₂O / 0 - 20 °C

4.1: dimethylformamide; tetrahydrofuran / 0 °C

5.1: 96 percent / (PCy₃)2Cl₂Ru=CHPh / CH₂Cl₂ / 20 °C

6.1: TFA / tetrahydrofuran / 20 °C

6.2: 98 percent / imidazole / dimethylformamide / 20 °C

7.1: m-CPBA; NaHCO₃ / CH₂Cl₂ / 0 - 20 °C

8.1: LiAlH₄ / diethyl ether / -20 °C

9.1: TBAI; NaH / tetrahydrofuran; dimethylformamide / 20 °C

9.2: 51 percent / CSA / methanol; tetrahydrofuran / 0 °C

10.1: 95 percent / iodine; PPh₃; imidazole / tetrahydrofuran / 20 °C

11.1: 90 percent / dimethylsulfoxide / 45 °C

12.1: DIBAL-H / CH₂Cl₂ / -95 °C

12.2: 83 percent / NaBH₄ / CH₂Cl₂; methanol / -20 - 20 °C

13.1: 95 percent / nBu₃P; pyridine / 20 °C

14.1: NCS / CH₂Cl₂; CCl₄ / 20 °C

15.1: 70 percent / AgOTf; 2,6-di-tert-butyl-4-methylpyridine; 4 Angstroem MS / CH₂Cl₂; CCl₄ / -90 - -15 °C

16.1: 93 percent / AgOTf; i-Pr₂NEt; 4 Angstroem MS / benzene / 20 °C

With pyridine; 1H-imidazole; N-chloro-succinimide; lithium aluminium tetrahydride; 2,6-di-tert-butyl-4-methylpyridine; tributylphosphine; 4 Angstroem MS; dihydrogen peroxide; iodine; silver trifluoromethanesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; Grubbs catalyst first generation; In tetrahydrofuran; tetrachloromethane; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2007.01.102