Technology Process of C32H25N3O2
There total 5 articles about C32H25N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzylidene phenylamine; acetic acid;
In
methanol; acetonitrile;
at 20 ℃;
for 0.5h;
DOI:10.1021/ol202080x
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / diethyl ether; hexane / 0.25 h / -70 °C / Inert atmosphere
1.2: 0.5 h / -70 °C / Inert atmosphere
2.1: potassium fluoride; palladium diacetate / methanol; PEG-400 / 1.5 h / 20 °C
3.1: hydrogen bromide; acetic acid / water / 40 °C / Inert atmosphere
4.1: benzylidene phenylamine; acetic acid / methanol; acetonitrile / 0.5 h / 20 °C
With
potassium fluoride; n-butyllithium; hydrogen bromide; palladium diacetate; benzylidene phenylamine; acetic acid;
In
methanol; PEG-400; diethyl ether; hexane; water; acetonitrile;
2.1: Suzuki coupling;
DOI:10.1021/ol202080x
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: bromine; sodium acetate; acetic acid / 80 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 0.25 h / -70 °C / Inert atmosphere
2.2: 0.5 h / -70 °C / Inert atmosphere
3.1: potassium fluoride; palladium diacetate / methanol; PEG-400 / 1.5 h / 20 °C
4.1: hydrogen bromide; acetic acid / water / 40 °C / Inert atmosphere
5.1: benzylidene phenylamine; acetic acid / methanol; acetonitrile / 0.5 h / 20 °C
With
potassium fluoride; n-butyllithium; hydrogen bromide; bromine; sodium acetate; palladium diacetate; benzylidene phenylamine; acetic acid;
In
methanol; PEG-400; diethyl ether; hexane; water; acetonitrile;
3.1: Suzuki coupling;
DOI:10.1021/ol202080x