1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

Base Information

Chemical Name:1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane
CAS No.:27491-80-1
Molecular Formula:C₁₄H₂₄Si₂
Molecular Weight:248.516
Hs Code.:

Synonyms:1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

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Chemical Property of 1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

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Technology Process of 1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

There total 6 articles about 1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 13528-93-3
1,2-bis-(chlorodimethylsilyl)ethane

: 27491-80-1
1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

Guidance literature:: With tetrabutylammonium perchlorate; In tetrahydrofuran; at 22 ℃; Inert atmosphere; Sealed tube; Electrolysis;
DOI:10.1021/jacs.0c10899

Reference yield:

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 27491-80-1
1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammonium perchlorate / tetrahydrofuran / 22 °C / Inert atmosphere; Sealed tube; Electrolysis

2: tetraethylammonium tosylate / 22 °C / Electrolysis; Inert atmosphere

3: tetrabutylammonium perchlorate / tetrahydrofuran / 22 °C / Inert atmosphere; Sealed tube; Electrolysis

With tetrabutylammonium perchlorate; tetraethylammonium tosylate; In tetrahydrofuran;
DOI:10.1021/jacs.0c10899

Reference yield:

: 2762-93-8
(1-phenylethane-1,2-diyl)bis(trimethylsilane)

: 27491-80-1
1,1,4,4-tetramethyl-2-phenyl-1,4-disilycyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: tetraethylammonium tosylate / 22 °C / Electrolysis; Inert atmosphere

2: tetrabutylammonium perchlorate / tetrahydrofuran / 22 °C / Inert atmosphere; Sealed tube; Electrolysis

With tetrabutylammonium perchlorate; tetraethylammonium tosylate; In tetrahydrofuran;
DOI:10.1021/jacs.0c10899