1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

Base Information

Chemical Name:1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole
CAS No.:1006726-70-0
Molecular Formula:C₄₁H₃₉N₅O₄
Molecular Weight:665.792
Hs Code.:

Synonyms:1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

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Chemical Property of 1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

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Technology Process of 1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

There total 1 articles about 1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006726-55-1
1,1',1''-tribenzyl-1H,1'H,1''H-[2,2';5',2'']-terpyrrole-5,5''-bis(carbaldehyde)

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 1006726-70-0
1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

Guidance literature:: With silica gel; triethylamine; In ethanol; at 20 ℃; for 2.5h;
DOI:10.1002/anie.200703258

Reference yield: 47.0%

: 1006726-70-0
1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole

: 963-16-6
(E)-1,2-bis(phenylsulfonyl)ethylene

: 1006726-82-4
1',1'',1'''-tribenzyl-5'''-(carbaldehyde)-5-(methoxycarbonyl)-1H,1'H,1''H,1'''H-[2,2';5',2'';5'',2''']-quaterpyrrole

: 1006726-57-3
1',1'',1'''-tribenzyl-5,5''''-bis(methoxycarbonyl)-1H,1'H,1''H,1'''H,1''''H-[2,2';5',2'';5'',2''';5''',2'''']-pentapyrrole

Guidance literature:: 1,1',1''-tribenzyl-2,5''-bis[(E)-(methoxycarbonyl)methyliminomethyl]-1H,1'H,1''H-[2,2';5',2'']-terpyrrole; (E)-1,2-bis(phenylsulfonyl)ethylene; With tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; triphenylphosphine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201000742