benzyl 4-methylpenta-2,3-dienote

Base Information

Chemical Name:benzyl 4-methylpenta-2,3-dienote
CAS No.:1373129-24-8
Molecular Formula:C₁₃H₁₄O₂
Molecular Weight:202.253
Hs Code.:

Synonyms:benzyl 4-methylpenta-2,3-dienote

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Chemical Property of benzyl 4-methylpenta-2,3-dienote

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Technology Process of benzyl 4-methylpenta-2,3-dienote

There total 3 articles about benzyl 4-methylpenta-2,3-dienote which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 15097-38-8
(carbobenzyloxymethylene)triphenylphosphorane

: 79-30-1
isobutyryl chloride

: 1373129-24-8
benzyl 4-methylpenta-2,3-dienote

Guidance literature:: isobutyryl chloride; With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

(carbobenzyloxymethylene)triphenylphosphorane; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol300550x

Reference yield:

: 5437-45-6
Benzyl bromoacetate

: 1373129-24-8
benzyl 4-methylpenta-2,3-dienote

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

With triethylamine; In dichloromethane; toluene;
DOI:10.1002/anie.201916471

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1373129-24-8
benzyl 4-methylpenta-2,3-dienote

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C

2: toluene / 20 °C

3: triethylamine / dichloromethane / 1 h / 20 °C

With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1002/anie.201916471