C₂₃H₃₁⁽²⁾HN₂Si

Base Information

Chemical Name:C₂₃H₃₁⁽²⁾HN₂Si
CAS No.:1383232-60-7
Molecular Formula:C₂₃H₃₂N₂Si
Molecular Weight:365.598
Hs Code.:

C<sub>23</sub>H<sub>31</sub><sup>(2)</sup>HN<sub>2</sub>Si

Synonyms:C₂₃H₃₁⁽²⁾HN₂Si

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Chemical Property of C₂₃H₃₁⁽²⁾HN₂Si

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Technology Process of C₂₃H₃₁⁽²⁾HN₂Si

There total 4 articles about C₂₃H₃₁⁽²⁾HN₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383232-54-9
N-(2-deuteriophenyl)-N-methyl-2-aminopyridine

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1383232-60-7
C₂₃H₃₁⁽²⁾HN₂Si

Guidance literature:: With bis(acetylacetonato)palladium(II); toluene-4-sulfonic acid; p-benzoquinone; In benzene; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.003

Reference yield:

: 1243273-04-2
N-(2-deuteriophenyl)-2-aminopyridine

: 1383232-60-7
C₂₃H₃₁⁽²⁾HN₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 12 h / 25 °C

2: bis(acetylacetonato)palladium(II); toluene-4-sulfonic acid; p-benzoquinone / benzene / 1 h / 80 °C / Inert atmosphere

With bis(acetylacetonato)palladium(II); potassium tert-butylate; toluene-4-sulfonic acid; p-benzoquinone; In N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2012.04.003

Reference yield:

: 109-04-6
2-bromo-pyridine

: 1383232-60-7
C₂₃H₃₁⁽²⁾HN₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,4-dioxane / 12 h / 100 °C / Inert atmosphere

2: potassium tert-butylate / N,N-dimethyl-formamide / 12 h / 25 °C

3: bis(acetylacetonato)palladium(II); toluene-4-sulfonic acid; p-benzoquinone / benzene / 1 h / 80 °C / Inert atmosphere

With bis(acetylacetonato)palladium(II); potassium tert-butylate; toluene-4-sulfonic acid; p-benzoquinone; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 1,4-dioxane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tet.2012.04.003