Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

Base Information

Chemical Name:Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide
CAS No.:75119-56-1
Molecular Formula:C₁₃H₁₃Cl₃N₂O₂
Molecular Weight:335.617
Hs Code.:

Synonyms:Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

Chemical Property:

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Technology Process of Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

There total 8 articles about Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 110-91-8,99108-56-2
morpholine

: 75119-50-5
1,2,2,2-tetrachloro-1-phenylethyl isocyanate

: 75119-56-1
Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃;

Reference yield:

: 25801-48-3
(2,2,2-Trichloro-1-isocyanato-ethyl)-benzene

: 75119-56-1
Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: Cl₂ / CCl₄ / 40 - 50 °C / Irradiation; other reagent (SO₂Cl₂)

2: 47 percent / triethylamine / diethyl ether / 0 °C

With chlorine; triethylamine; In tetrachloromethane; diethyl ether;

Reference yield:

: 25801-35-8
(2,2,2-Trichloro-1-phenyl-ethyl)-carbamic acid methyl ester

: 75119-56-1
Morpholine-4-carboxylic acid [2,2,2-trichloro-1-phenyl-eth-(E)-ylidene]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / CCl₄ / 70 - 80 °C / Irradiation; other reagent (SO₂Cl₂)

2: 91 percent / PCl₅ / 100 - 110 °C

3: 47 percent / triethylamine / diethyl ether / 0 °C

With phosphorus pentachloride; chlorine; triethylamine; In tetrachloromethane; diethyl ether;