[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

Base Information

Chemical Name:[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene
CAS No.:599173-62-3
Molecular Formula:C₂₅H₄₈O₅Si₂
Molecular Weight:484.824
Hs Code.:

[3-(<i>tert</i>-butyl-dimethyl-silanyloxy)-1-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

Synonyms:[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

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Chemical Property of [3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

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Technology Process of [3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

There total 4 articles about [3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 107-30-2
chloromethyl methyl ether

: 109613-56-1
(2S,3S)-(+)-3-benzyloxy-1,4-bis(tert-butyl-dimethyl-silyloxy)butan-2-ol

: 599173-62-3
[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 0 - 20 ℃; for 30h;
DOI:10.1016/S0040-4020(03)00692-6

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 599173-62-3
[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / p-TsOH / 8 h

2: 81.5 percent / LiALH₄; AlCl₃ / diethyl ether; CH₂Cl₂ / -20 - 50 °C

3: 78 percent / imidazole / dimethylformamide / -20 - 20 °C

4: 86 percent / iPr₂NEt / 30 h / 0 - 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; aluminium trichloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00692-6

Reference yield:

: 38270-72-3
dimethyl 2,3-O-benzylidene-L-tartrate

: 599173-62-3
[3-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-methoxymethoxy-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 81.5 percent / LiALH₄; AlCl₃ / diethyl ether; CH₂Cl₂ / -20 - 50 °C

2: 78 percent / imidazole / dimethylformamide / -20 - 20 °C

3: 86 percent / iPr₂NEt / 30 h / 0 - 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; aluminium trichloride; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00692-6