(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

Base Information

Chemical Name:(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol
CAS No.:1574347-73-1
Molecular Formula:C₁₈H₂₇N₃O₉
Molecular Weight:429.427
Hs Code.:

Synonyms:(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

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Technology Process of (1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

There total 1 articles about (1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 1072-86-2,1460-57-7,1792-81-0,54383-22-1,57794-08-8,931-17-9
(1R,2R)-trans-1,2-cyclohexanediol

: 145840-43-3
3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-glucopyranosyl trichloroacetimidate

: 1574347-72-0
(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl)cyclohexanediol

: 1574347-73-1
(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at 20 ℃; for 2h; Molecular sieve; Inert atmosphere;
DOI:10.1039/c3ob42164c

Reference yield: 80.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 1574347-73-1
(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

: 1574348-15-4
1R,2R-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-O-(tertbutyldimethylsilyl)-cyclohexanediol

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3ob42164c

Reference yield: 41.0%

: 1574347-73-1
(1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol

: triethylammonium n-octadecyl hydrogenphosphonate

: 1574348-14-3
triethylammonium (1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol 2-(n-octadecylphosphate)

Guidance literature:: (1R,2R)-1-O-(2-azido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)cyclohexanediol; triethylammonium n-octadecyl hydrogenphosphonate; With pyridine; pivaloyl chloride; at 20 ℃; for 2h; Inert atmosphere;

With iodine; In water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3ob42164c