2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

Base Information

• Chemical Name: 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol
• CAS No.: 1202532-55-5
• Molecular Formula: C₆₁H₆₂O₁₀
• Molecular Weight: 955.157

Synonyms:2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

Chemical Property of 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

Chemical Property:

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Technology Process of 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

There total 1 articles about 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C61H63ClO10 (173325-22-9) → 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol (1202532-55-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In acetonitrile; at 85 ℃; for 2h; Molecular sieve;

DOI:10.1021/jo901945e

Reference yield: 75.0%

chloroform (67-66-3,8013-54-5) + 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol (1202532-55-5) → C62H62Cl2O10 (1202532-59-9)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; at 20 ℃; for 24h;

DOI:10.1021/jo901945e

upstream raw materials:

C₆₁H₆₃ClO₁₀

Downstream raw materials:

C₆₂H₆₂Cl₂O₁₀

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