[6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol

Base Information

• Chemical Name: [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol
• CAS No.: 874770-89-5
• Molecular Formula: C₁₄H₁₈O₆
• Molecular Weight: 282.293

Synonyms:[6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol

Chemical Property of [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol

Chemical Property:

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Technology Process of [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol

There total 2 articles about [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl ribofuranoside (1824-96-0,1824-97-1,3795-68-4,3795-69-5,4229-54-3,5531-18-0,7473-45-2,13039-63-9,13039-64-0,13039-65-1,13039-67-3,22416-73-5,22861-09-2,25129-51-5,52485-92-4,52689-55-1,52689-56-2,56607-40-0,72880-70-7,79083-42-4,86782-30-1,86782-31-2,89615-03-2,89673-67-6,89707-99-3,102045-32-9,135910-17-7) + p-Anisaldehyde dimethyl acetal (2186-92-7) → [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol (874770-89-5)

Guidance literature:

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 45 - 55 ℃; for 6h;

DOI:10.1021/ol0524048

Reference yield:

D-Ribose (532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7) → [6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol (874770-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄

2: 5 g / TsOH*H₂O / dimethylformamide / 6 h / 45 - 55 °C

With sulfuric acid; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;

DOI:10.1021/ol0524048

Reference yield: 99.0%

[6-methoxy-2-(4-methoxyphenyl)tetrahydrofuro[3,4-d][1,3]-dioxol-4-yl]methanol (874770-89-5) + N-tert-butoxycarbonyl aspartic acid tert-butyl ester (34582-32-6) → 2-tert-butoxycarbonylamino-succinic acid 1-tert-butyl ester 4-[6-methoxy-2-(4-methoxy-phenyl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester (874770-90-8)

Guidance literature:

With dmap; benzoyl chloride; triethylamine; In tetrahydrofuran; for 24h;

DOI:10.1021/ol0524048

upstream raw materials:

methyl ribofuranoside

p-Anisaldehyde dimethyl acetal

D-Ribose

Downstream raw materials:

2-tert-butoxycarbonylamino-succinic acid 1-tert-butyl ester 4-[6-methoxy-2-(4-methoxy-phenyl)-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl] ester

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