3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

Base Information

Chemical Name:3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine
CAS No.:1319017-28-1
Molecular Formula:C₄₂H₃₄N₂
Molecular Weight:566.745
Hs Code.:

Synonyms:3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

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Chemical Property of 3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

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Technology Process of 3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

There total 6 articles about 3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1319017-25-8
2-chloro-9,9-dimethyl-10-phenyl-9,10-dihydroacridine

: 1307793-50-5
8,8-dimethyl-8H-indolo[3,2,1-de]acridin-3-ylboronic acid

: 1319017-28-1
3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

Guidance literature:: With sodium carbonate; palladium diacetate; tris-(o-tolyl)phosphine; In 1,4-dioxane; water; toluene; for 16h; Reflux;

Reference yield:

: 918163-16-3
2-[2-(4-chlorophenylamino)phenyl]propan-2-ol

: 1319017-28-1
3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanesulfonic acid / toluene / 2 h / 20 - 50 °C

2.1: toluene / 1 h / Inert atmosphere

2.2: 1 h / Reflux

3.1: sodium carbonate / palladium diacetate; tris-(o-tolyl)phosphine / toluene; 1,4-dioxane; water / 16 h / Reflux

With methanesulfonic acid; sodium carbonate; palladium diacetate; tris-(o-tolyl)phosphine; In 1,4-dioxane; water; toluene; 2.1: Ullmann Reaction;

Reference yield:

: 1224892-52-7
3-bromo-8,8-dimethyl-8H-indolo [3,2,1-de]acridine

: 1319017-28-1
3-(9,9-Dimethyl-10-phenyl-9,10-dihydroacridin-2-yl)-8,8-dimethyl-8H-indolo[3,2,1-de]acridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / cyclohexane; tetrahydrofuran / 1 h / -70 °C

1.2: 1 h / 20 °C

2.1: sodium carbonate / palladium diacetate; tris-(o-tolyl)phosphine / toluene; 1,4-dioxane; water / 16 h / Reflux

With n-butyllithium; sodium carbonate; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; 1,4-dioxane; cyclohexane; water; toluene;