tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

Base Information

Chemical Name:tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane
CAS No.:133508-97-1
Molecular Formula:C₃₅H₄₂O₄P₄
Molecular Weight:650.611
Hs Code.:

Synonyms:tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

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Technology Process of tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

There total 5 articles about tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 133508-95-9,133576-66-6
dibromure d'hexaphenyl-1,1,5,5,9,12 dioxo-9,12 diphosphona-9,12 diphosphonia-1,5 cyclopentadecane

: 133508-97-1
tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

Guidance literature:: With sodium hydroxide; In ethanol; for 12h; Heating;
DOI:10.1016/S0040-4020(01)90498-3

Reference yield:

: 18899-64-4
1,2-Bis(phenylphosphino)ethane

: 133508-97-1
tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: AIBN / 1 h at 0 deg C, then 24 h at 75 deg C

2: 75 percent / brome / CH₂Cl₂ / 24 h / Ambient temperature

3: 50 percent / toluene / 120 h / Heating

4: 75 percent / aq. NaOH / ethanol / 12 h / Heating

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); bromine; In ethanol; dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)90498-3

Reference yield:

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 133508-97-1
tetraphenyl-1,4,8,12 tetraoxo-1,4,8,12 tetraphospha-1,4,8,12 cyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / toluene / 120 h / Heating

2: 75 percent / aq. NaOH / ethanol / 12 h / Heating

With sodium hydroxide; In ethanol; toluene;
DOI:10.1016/S0040-4020(01)90498-3