(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

Base Information

Chemical Name:(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid
CAS No.:108194-33-8
Molecular Formula:C₁₉H₂₆O₆
Molecular Weight:350.412
Hs Code.:

Synonyms:(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

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Chemical Property of (2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

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Technology Process of (2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

There total 4 articles about (2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3066-90-8
2,3-dimethoxy-5-methylbenzene-1,4-diol

: 26187-80-4
2,6-trans-2,6-dimethyl-8-hydroxy-2,6-octadienoic acid

: 108194-33-8
(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane; diethyl ether; for 2h; Ambient temperature;
DOI:10.1248/cpb.33.3182

Reference yield:

: 605-94-7
2,3-Dimethoxy-5-methyl-1,4-benzoquinone

: 108194-33-8
(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂S₂O₄ / diethyl ether

2: 45percent BF₃*Et₂O / dioxane; diethyl ether / 2 h / Ambient temperature

With sodium dithionite; boron trifluoride diethyl etherate; In 1,4-dioxane; diethyl ether;
DOI:10.1248/cpb.33.3182

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 108194-33-8
(2E,6E)-8-(2,5-Dihydroxy-3,4-dimethoxy-6-methyl-phenyl)-2,6-dimethyl-octa-2,6-dienoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / SeO₂ / ethanol / 1 h / Heating

2: AgNO₃/2 N NaOH / ethanol; H₂O / 3 h / Ambient temperature

3: 45percent BF₃*Et₂O / dioxane; diethyl ether / 2 h / Ambient temperature

With sodium hydroxide; selenium(IV) oxide; boron trifluoride diethyl etherate; silver nitrate; In 1,4-dioxane; diethyl ether; ethanol; water;
DOI:10.1248/cpb.33.3182